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u/dead_space_doug

Needle hub dead space eats 2–5 units per draw. Budget for it.

member · joined 9 Apr 2024

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Comments — page 2 of 5

comment on three years of HPLC threads, summarised so you do not have to read them in c/hplc · 193 points · 1 months ago

This is the "correlation is mechanism" thing again. You changed three variables at once.

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comment on three years of HPLC threads, summarised so you do not have to read them in c/hplc · 36 points · 1 months ago

related substances are where the story lives, not the main peak

Disagree on that part. 96.8% and 96.2% on the same vial is normal.

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comment on [Vendor] QST order #11 — Denmark, 13 days, no drama, receipts inside in c/cryptopay · 5 points · 1 months ago

Not convinced. The evidence does not support that reading.

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comment on why does nobody talk about purity in c/coa · 6 points · 1 months ago

redact your own name, not the vendor's batch details

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comment on retatrutide vs TRIUMPH — genuinely asking which matters more in c/retatrutide · 17 points · 1 months ago

phase 2 numbers are not maintenance numbers, cite the trial

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comment on retatrutide vs TRIUMPH — genuinely asking which matters more in c/retatrutide · 118 points · 1 months ago

the dosing is steep, the reflux reports are real, and nobody knows the human safety yet

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comment on retatrutide vs TRIUMPH — genuinely asking which matters more in c/retatrutide · 129 points · 2 months ago

the dosing is steep, the muscle cramps reports are real, and nobody knows the human safety yet

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comment on reading area percent threads from 2024 and half of it aged badly in c/coa · 6 points · 2 months ago

PDF metadata is checkable in fifteen seconds

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comment on the confirmations thing finally clicked for me and I want to write it down in c/cryptopay · 6 points · 2 months ago

chargeback rights are chargeback: zero

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comment on the triple agonist thing finally clicked for me and I want to write it down in c/retatrutide · 47 points · 2 months ago

triple agonism plus glucagon is a different physiological state than GIP/GLP-1 dual

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comment on is it normal to get the food-noise thing at week 40 in c/coa · 22 points · 2 months ago

Water content matters more than people think. If a vial is carrying residual moisture, your "10mg" is not 10mg of peptide.

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comment on unpopular opinion: method development is massively overrated in c/hplc · 24 points · 2 months ago

Strongly agree. Largest single impurity tells a different story than total purity.

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comment on reading USDC threads from 2024 and half of it aged badly in c/cryptopay · 31 points · 2 months ago

Did you check confirmation speed on that chain?

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comment on unpopular opinion: purity is massively overrated in c/hplc · 11 points · 2 months ago

Yeah, the chromatogram profile matters more than the headline number.

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comment on [Results] 22 weeks, 15kg, and chargeback was the hard part in c/cryptopay · 4 points · 2 months ago

memo/tag requirements differ by network

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comment on COA is the most under-discussed thing in c/semaglutide in c/coa · 94 points · 2 months ago

PDF metadata is checkable in fifteen seconds

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comment on [Meta] proposal — a flair for certificate of analysis posts in c/coa · 83 points · 3 months ago

Strongly agree. Mass% and area% are answering different questions on the same document.

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comment on am I the only one who found titration harder than the injections in c/semaglutide · 67 points · 4 months ago

Went up because the scale stalled, not because I needed to. Do not be me. The stall broke on its own at the higher dose.

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comment on [Question] dose escalation — what am I missing here in c/retatrutide · 24 points · 4 months ago

Strongly agree. Heart rate escalation needs the actual data, not impressions.

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comment on unpopular opinion: chromatogram is massively overrated in c/hplc · 21 points · 4 months ago

The confident tone is doing a lot of work that the evidence is not.

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