is it normal to get early fullness at week 14
Confession thread, sort of. I went from 2.5mg to 1.0mg much faster than I should have because the scale had stalled and I got impatient. The stall broke about 4 weeks later, at which point I had no way of knowing whether the dose increase did anything or whether it would have broken anyway. So now I have sulphur…
Retitled to remove editorialising. Put the evidence in the body.
Mechanistically the bit that matters is purity. It explains most of the early profile and a decent chunk of the outcome.
Yeah, 96.8% area is not the problem, the missing impurity breakdown is the problem.
chromatogram or it did not happen
Yeah, 96.8% area is not the problem, the missing impurity breakdown is the problem.
area% is not mass%, and here is exactly why it matters
Retitled to remove editorialising.
Yes, exactly this, and it is the bit that took me 87 weeks to accept.
Disagree. What you are describing is consistent with batch, not with what you concluded.