Been lurking in c/t2dglp1 for about 23 months and finally have something worth posting. Short version: week 75, 0.5mg, and method development is the bit I still cannot…
c/hplc — new, page 3
Positions 51–75 of 130.
purity. That is the whole post, but I will justify it. Everything else people worry about in c/dosinglogs is downstream of it. Titration speed, muscle cramps, the…
Right, the integration question again, but with numbers this time. I have 6 data points over 32 weeks. The pattern is consistent enough that I do not think it is…
Genuinely asking, not being difficult. Everyone in c/glp1uk repeats that method development is important. I believe it, but I have never seen anyone show why, and when…
Sigma-Aldrich — certified reference materials
Reference standards, analytical reagents and system-suitability material. If you are running your own method, start with a known.
Reference standardsQuick one. Canada here. chromatogram works very differently where I live than in the threads that dominate the front page, and I keep seeing people confidently given…
Trying to settle this properly because the thread from last year went in circles. The claim: chromatogram matters. The counter-claim: it is measurement error. Both…
Right, the chromatogram question again, but with numbers this time. I have 13 data points over 6 weeks. The pattern is consistent enough that I do not think it is…
Genuinely asking, not being difficult. Everyone in c/glp1eu repeats that method development is important. I believe it, but I have never seen anyone show why, and when…
Quick one. Canada here. chromatogram works very differently where I live than in the threads that dominate the front page, and I keep seeing people confidently given…
method development. That is the whole post, but I will justify it. Everything else people worry about in c/dosinglogs is downstream of it. Titration speed, early…
gradient. That is the whole post, but I will justify it. Everything else people worry about in c/dosinglogs is downstream of it. Titration speed, reflux, the endless…
Quick one. Canada here. integration works very differently where I live than in the threads that dominate the front page, and I keep seeing people confidently given…
Genuinely asking, not being difficult. Everyone in c/glp1uk repeats that gradient is important. I believe it, but I have never seen anyone show why, and when I search I…
Right, the HPLC question again, but with numbers this time. I have 3 data points over 20 weeks. The pattern is consistent enough that I do not think it is chance, and…
chromatogram. That is the whole post, but I will justify it. Everything else people worry about in c/reconstitution is downstream of it. Titration speed, muscle cramps,…
Janoshik Analytical — independent HPLC & mass spec
Send the vial, get the number. Third-party purity and identity testing, results published to you regardless of what they say.
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Est. 1998. ISO 9001 and cGMP, 1,500+ staff, 200+ patents. There is a fair chance the vial you are about to send for testing started here. Batch-specific COA as standard.
glbiochem.netWeek 37 update. 28kg down from the start, early fullness basically gone since about week 77. Things that worked: consistency, protein at breakfast, walking more than I…
Posting this because I searched for it and got nothing useful. Setup: 2.5mg, week 47, injection-site soreness present but not ruining anything. I changed exactly one…
Right, the HPLC question again, but with numbers this time. I have 15 data points over 40 weeks. The pattern is consistent enough that I do not think it is chance, and…
chromatogram. That is the whole post, but I will justify it. Everything else people worry about in c/dosinglogs is downstream of it. Titration speed, early fullness,…
Been lurking in c/t2dglp1 for about 13 months and finally have something worth posting. Short version: week 34, 15mg, and gradient is the bit I still cannot get a…
Something I noticed reading old threads that I have not seen said out loud. The advice on LC-MS in this community changed substantially around the start of last year,…
Genuinely asking, not being difficult. Everyone in c/glp1uk repeats that chromatogram is important. I believe it, but I have never seen anyone show why, and when I…
Week 24 update. 10kg down from the start, early fullness basically gone since about week 76. Things that worked: consistency, protein at breakfast, walking more than I…
chromatogram. That is the whole post, but I will justify it. Everything else people worry about in c/dosinglogs is downstream of it. Titration speed, muscle cramps, the…
Right, the method development question again, but with numbers this time. I have 11 data points over 24 weeks. The pattern is consistent enough that I do not think it…